New PDF release: Advances in Protein Chemistry, Vol. 5

By M.L. Anson, John T. Edsau (Eds.)

ISBN-10: 0120342057

ISBN-13: 9780120342051

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114-1 15 (277) 74-75 (16) be obtained in crystalline form by the procedure described by Bergmann and Zervas (74), although some workers have encountered difficulty in crystallizing this substance without inoculation with seed crystals. The chloride is best used immediately after its preparation, a small sample being set aside under petroleum ether for the inoculation of the next preparation. With regard to the attachment of an alanyl residue to an amino acid or peptide, the bromopropionyl bromide (or chloride) method of Fischer is feasible only when Dcalanyl peptides are desired.

M. , "C. ) 64-65 (282a) 113-115 (164) 125-126 (43) chucinamide acetate. . . . . . . . . . . . . . chucinamide HCl. . . . ... 230-237 (276a) chucine-N-carbonic acid anhydride. . . . . . . . 76. Ei-78 (301) Dchuche-N-carbonic acid anhydride. . . . . . . 48-50 (229) Acetyldehydroleucine. . . . Acetyldehydroleucylglycine. . . . . . 130-132 (115) Bencoyl-cleucinamide. Benzoyl-Dcleucinamide. . . ............. 171 (244) Bencoyl-cleucinhydrazide.

19 16 18 20 18 22 14 18 25 19 ... 25 16 27 ... 18 18 ... I%, H i 0 I%, H s 0 I%, H i 0 + 1eq. HC + 1eq. HC + 1eq. HC + 1eq. HC Ref. 148 166 166 148 148 156 156 193 193 193 74 248 197 288 77 204 157 283 78 187 283 283 283 139,276a 283 193 227a 74 274 88 202 289 224 202,291 202 245 245 203 203 45 SYNTHESIS OF PEPTIDEB ethyl ester to give the a rather than the y compound as the principal product. CHrCO &HI I C~H'CHXOCO-NHCHCO '+ 0 ' NHxCHXCOOCIH'+ CHrCOOH ~ H x CeHrCHaOCO-NH HCO-NHCHaCOOCxH' It is of interest that, in the reaction with Gtyrosine ethyl ester (88) Gglutamic acid diethyl ester (74), or Gcysteine benzyl ester (203), the major products are also derivatives of the a-peptides.

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Advances in Protein Chemistry, Vol. 5 by M.L. Anson, John T. Edsau (Eds.)


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